Reaktion #465571

Reaktionsgleichung

N-phenyl-o-phenylenediamine

3,4,5-trimethoxybenzoyl chloride

→

N-[(3,4,5-trimethoxyphenyl)carbonyl]-N'-phenyl-phenylenediamine

Lösungsmittel

diethyl ether

diethyl ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONwas added dropwise
2. 2
   SonstigeThe solvents were then removed in vacuo

Vorschrift

A solution of N-phenyl-o-phenylenediamine (1.84 g, 10 mmol) in diethyl ether (90 ml) was stirred at room temperature as 3,4,5-trimethoxybenzoyl chloride (2.31 g, 10 mmol) in diethyl ether (40 ml) was added dropwise. The reaction mixture was then stirred overnight at room temperature. The solvents were then removed in vacuo leaving N-[(3,4,5-trimethoxyphenyl)carbonyl]-N'-phenyl-phenylenediamine.

Quelle