Reaktion #464214

ord-6b7cafded22f44a094fa3a0bcef386ed

Reaktionsgleichung

CC(=O)c1cccc(N)c1
3-aminoacetophenone
O=C(Cl)CCCC(=O)Cl
glutaryl dichloride
→
CC(=O)c1cccc(NC(=O)CCCC(=O)Nc2cccc(C(C)=O)c2)c1
N,N'-bis(3-acetylphenyl)pentanediamide

Edukte

CC(=O)c1cccc(N)c1
3-aminoacetophenone
O=C(Cl)CCCC(=O)Cl
glutaryl dichloride
—
N,N'-bis(3,5-diacetylphenyl)(isophthalic acid diamide)

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

N,N'-bis(3,5-diacetylphenyl)(isophthalic acid diamide), mp 283-4° C. Also analogously, N,N'-bis(3-acetylphenyl)pentanediamide, mp 174-5° C. was prepared from 3-aminoacetophenone and glutaryl dichloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06022900uspto-grants-2000_02