Reaktion #463735

Reaktionsgleichung

iodomethane

2,3-diaminonapthalene

4,5-dimethyl-1,2-benzoquinone

phenazine

→

2,3-dimethylbenzo(B)phenazine

Lösungsmittel

acetic acid

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturat reflux for 2 hours

Vorschrift

The 2,3-dimethylbenzo(B)phenazine was prepared by the condensation of 2,3-diaminonapthalene with 4,5-dimethyl-1,2-benzoquinone in 4:1 ethanol to acetic acid at reflux for 2 hours. The phenazine was alkylated by the procedure of Synthesis Example 8, using iodomethane. Electrochemical analysis was consistent with an N,N'-dialkylated phenazine.

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