Reaktion #463593

Reaktionsgleichung

1,2-O-Dioleyl-3-O-tritylglycerol

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title compound

Ausbeute 87.0%

1,2-O-dioleylglycerol

Ausbeute 87.0%

Lösungsmittel

trichloroacetic acid methylene chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   WaschenThe organic layer was then washed with saturated aqueous sodium hydrogen carbonate solution and water
2. 2
   Sonstigedried
3. 3
   Einengenconcentrated
4. 4
   SonstigeThe residue was purified by column chromatography (silica gel/chloroform)

Vorschrift

1,2-O-Dioleyl-3-O-tritylglycerol (6.10 g, 7.3 mmol) was reacted with 5% trichloroacetic acid/methylene chloride (50 ml, w/v) at ambient temperature for 1 hour. The organic layer was then washed with saturated aqueous sodium hydrogen carbonate solution and water, dried, and concentrated. The residue was purified by column chromatography (silica gel/chloroform) to provide 3.75 g (87%) of the title compound.

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