Reaktion #46036

ord-38acc37f71194bc68117a8b34688af43

Reaktionsgleichung

CCCCOCCO
DOWANOL
CCCCCCCCn1sc(Cl)c(Cl)c1=O
DCOIT
COC(C)COC(C)CO
DOWANOL DPM
→
CCCCCCCCn1sc(Cl)c(Cl)c1=O.COC(C)COC(C)CO
DCOIT Dowanol DPM

Edukte

CCCCOCCO
DOWANOL
CCCCCCCCn1sc(Cl)c(Cl)c1=O
DCOIT
COC(C)COC(C)CO
DOWANOL DPM

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

In the DOWANOL PPH preparation above, substitute 18 g of 25% DCOIT in DOWANOL DPM (final concentration of 1500 ppm DCOIT) stirring as directed.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07740906B2uspto-grants-2010_06