Reaktion #457572

Reaktionsgleichung

5,5-dimethyl-1,3-cyclohexanedione

palmitoyl chloride

triethylamine

→

desired product

Ausbeute 67.0%

3-palmitoyloxy-2-(4'-methylphenyl)-5,5-dimethyl-2-cyclohexenone

Ausbeute 67.0%

Lösungsmittel

methylene chloride

Reaktionsbedingungen

Vorschrift

Using the procedure described in Example III and starting with 3.00 g (0.0130 mol) of 2-4'-methylphenyl)-5,5-dimethyl-1,3-cyclohexanedione, 2.69 g (0.0098 mol) of palmitoyl chloride, 2.63 g (0.0260 mol) of triethylamine, and 30 ml of methylene chloride, 3.1 g (67% yield) of a clear, colorless oil was obtained as the desired product.

Quelle