Reaktion #454103

Reaktionsgleichung

benzoic acid

2,2-bis(4-hydroxyphenyl)-1,1,1,3,3,3-hexafluoropropane

→

1,1,1,3,3,3-hexafluoropropane

Ausbeute 89.0%

Reaktionsbedingungen

Vorschrift

A reaction was conducted as described in Example 6 except that benzoic acid was replaced with 105 mmol of 2,2-bis(4-hydroxyphenyl)-1,1,1,3,3,3-hexafluoropropane and the amount of PGE was 200 mmol. Desired 2,2-bis[4-(2-hydroxy-3-phenoxypropyloxy)phenyl[-1,1,1,3,3,3-hexafluoropropane was formed in analytical yield of 89% and isolated in a yield of 83%.

Quelle