Reaktion #45250

ord-daf586578e2247f893ac7b467e223462

Reaktionsgleichung

CCOC(=O)CBr
Ethyl bromoacetate
O=[N+]([O-])c1cccc(O)c1
meta-nitrophenol
CCOC(=O)COc1cccc([N+](=O)[O-])c1
ethyl 2-(3-nitrophenoxy)acetate

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Ethyl bromoacetate is reacted with meta-nitrophenol under standard conditions to afford ethyl 2-(3-nitrophenoxy)acetate, which is elaborated to ethyl 2-(3-hydrazinophenoxy)acetate using the reduction/oxidation sequence described for Example Y.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07737283B2uspto-grants-2010_06