Reaktion #452412
ord-492df67242dd46b4a16e440148d080a3
Reaktionsgleichung
HMDI
cyclohexyl isocyanate
→
CHI
carbodiimide
HMDI
Reagenzien
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1Sonstigewere subjected to a reaction at 185° C. for 19 hours while nitrogen
- 2Sonstigewas bubbled
Vorschrift
To a mixture of 236 g of HMDI with 25.0 g of cyclohexyl isocyanate (referred to hereinafter as CHI) was added 2.60 g of the carbodiimidization catalyst, and they were subjected to a reaction at 185° C. for 19 hours while nitrogen was bubbled thereinto, to obtain a carbodiimide resulting from HMDI and CHI (degree of polymerization=10).