Reaktion #45199

Reaktionsgleichung

5-chloro-2-nitrobenzoic acid

dimethylamine

→

5-dimethylamino-2-nitrobenzoic acid

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturheated

Vorschrift

Concretely, 5-chloro-2-nitrobenzoic acid is dissolved in a dimethylamine aqueous solution and heated to produce 5-dimethylamino-2-nitrobenzoic acid. Hydrochloric acid is added to the reaction solution to precipitate out the product as a solid material. The solid material is separated to obtain 5-dimethylamno-2-nitrobenzoic acid almost quantitatively.

Quelle