Reaktion #449656

ord-1115f63737674e86ba475dd5b5e8555d

Reaktionsgleichung

COC(=O)CCCCCBr
methyl 6-bromohexanoate
CNCC(=O)O
methyl glycine
[H-].[Na+]
sodium hydride
O=C(O)CCCCCNCC(=O)O
6-[(carboxymethyl)amino]hexanoic acid

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

In this reaction scheme, methyl 6-bromohexanoate is alkylated with methyl glycine in the presence of sodium hydride to afford the 6-[(carboxymethyl)amino]hexanoic acid. Treatment of 6-[(carboxymethyl)amino]hexanoic acid with sodium hydroxide affords the corresponding 6-[(carboxymethyl)amino]hexanoic acid disodium salt.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05869527uspto-grants-1999_02