Reaktion #44840

ord-b9d79720df6a4456b06914d23a4f9fdc

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 4-fluorophenylenediamine and 1-isothiocyanato-1,2,3,4-tetrahydronaphthalene by Procedure D. The title compound was isolated by column chromatography as the free base and as a mixture of enantiomers (solid, mp 220-221° C.). MS(ES+) m/z 282 ([M+1]+, 100).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07737167B2uspto-grants-2010_06