Reaktion #44837

ord-eed1159a40e24904984eac4e15d275ed

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 3,5-bis(trifluoromethyl)-1,2-diaminobenzene and 1-isothiocyanato-1,2,3,4-tetrahydronaphthalene by Procedure D. The title compound was isolated by column chromatography as the free base and as a mixture of enantiomers (solid, dec. >240° C.). MS(ES+) m/z 400 ([M+1]+, 100).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07737167B2uspto-grants-2010_06