Reaktion #44834

Reaktionsgleichung

2-chlorobenzimidazole

(R)-1,2,3,4-tetrahydro-l-naphthylamine

→

title compound

(R)-N-(Benzimidazol-2-yl)-1,2,3,4-tetrahydro-1-naphthylamine

HCl

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe product was filtered off
2. 2
   Waschenwashed with acetonitrile

Vorschrift

The title compound was prepared from 2-chlorobenzimidazole and (R)-1,2,3,4-tetrahydro-l-naphthylamine by Procedure A (40 min at 170° C.). The product was filtered off and washed with acetonitrile to give the title compound as a HCl salt (white solid, mp 264-265° C.). MS(ES+) m/z 264 ([M+1]30, 100).

Quelle