Reaktion #446146

ord-f63adfa9e53c40b189810bceb6c9bd4b

Reaktionsgleichung

O=C(C1NCCc2sccc21)N1CCCCC1
4-(piperidin-1-yl)carbonyl-4,5,6,7-tetrahydrothieno[3,2-c]pyridine
[Al+3].[H-].[H-].[H-].[H-].[Li+]
lithium aluminium hydride
→
c1cc2c(s1)CCNC2CN1CCCCC1
4-(piperidin-1-yl)methyl-4,5,6,7-tetrahydrothieno[3,2-c]pyridine

Edukte

O=C(C1NCCc2sccc21)N1CCCCC1
4-(piperidin-1-yl)carbonyl-4,5,6,7-tetrahydrothieno[3,2-c]pyridine
[Al+3].[H-].[H-].[H-].[H-].[Li+]
lithium aluminium hydride

Reagenzien

Keine

Lösungsmittel

C1CCOC1
THF

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigePrepared as Description No

Vorschrift

Prepared as Description No. 4, from 1.7 g (6.8 mmoles) of 4-(piperidin-1-yl)carbonyl-4,5,6,7-tetrahydrothieno[3,2-c]pyridine and 600 mg (15.79 mmoles) of lithium aluminium hydride in 50 ml of dry THF.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04999359uspto-grants-1991_03