Reaktion #44389

ord-ffb9776517e246d191b666a66a7c7ed0

Reaktionsgleichung

O=C(O)c1ccc(Br)cc1F
4-bromo-2-fluorobenzoic acid
CCN.Cl
ethylamine hydrochloride
→
CCNC(=O)c1ccc(Br)cc1F
sub-title compound
CCNC(=O)c1ccc(Br)cc1F
4-bromo-N-ethyl-2-fluoro-benzamide

Edukte

O=C(O)c1ccc(Br)cc1F
4-bromo-2-fluorobenzoic acid
CCN.Cl
ethylamine hydrochloride

Reagenzien

Keine

Lösungsmittel

CCN(CC)CC
triethylamine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The sub-title compound was prepared by the method of example 18 step a) using 4-bromo-2-fluorobenzoic acid, ethylamine hydrochloride and triethylamine.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07737135B2uspto-grants-2010_06