Reaktion #443412

ord-dc91a8f4ff194edab2501f283e58eb17

Reaktionsgleichung

CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1
isophorone diisocyanate
OCCOCCOCCO
triethylene glycol
C=CC(=O)OCCO
2-hydroxyethyl acrylate
C=CC(=O)O.CCOC(N)=O
urethane acrylate

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

2 moles of isophorone diisocyanate, 1 mole of triethylene glycol, and 2 moles of 2-hydroxyethyl acrylate were reacted by a predetermined method so as to yield urethane acrylate as a monomer of a ultraviolet-curing resin. Subsequently, a monomeric composition was prepared by mixing 50 grams of the urethane acrylate, 25 grams of the acrylic ester compound obtained in Example 1, 25 grams of 1,6-hexanediol diacrylate as a monomer of the ultraviolet-curing resin, and 3 grams of benzylmethyl ketal as a photopolymerization initiator (produced by Ciba-Geigy and marketed under the trade name "Irgacure 651").

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05834576uspto-grants-1998_11