Reaktion #443403

Reaktionsgleichung

oxetane

delta-valerolactone

triethylaluminum water

→

delta-valerolactone oxetane

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONwere mixed
2. 2
   Sonstigepolymerized in a bulk state at 60° C. for 24 hours

Vorschrift

According to the ratio for charging as described in Table 2, oxetane and delta-valerolactone (referred to as VL in Table and Figure) were mixed, and polymerized in a bulk state at 60° C. for 24 hours using 0.2% by mol of a triethylaluminum-water (1/0.75) based complex as an initiator based on the total amount of the monomers.

Quelle