Reaktion #443248

Reaktionsgleichung

6-Chloro-5-ethylthioindoline

3-pyridylisocyanate

→

title compound

Ausbeute 48.0%

6-Chloro-5-ethylthio-1-(3-pyridylcarbamoyl)indoline

Ausbeute 48.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe crude product was recrystallised from ethanol/diethyl ether

Vorschrift

6-Chloro-5-ethylthioindoline (D64) (0.18 g, 0.85 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The crude product was recrystallised from ethanol/diethyl ether to give the title compound (0.14 g, 48%) as a white crystalline solid m.p.=225°-226° C.

Quelle