Reaktion #443247

Reaktionsgleichung

6-Chloro-5-vinylindoline

3-pyridylisocyanate

→

title compound

6-Chloro-5-vinyl-1-(3-pyridylcarbamoyl)indoline

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe crude product was recrystallised from ethanol/diethyl ether

Vorschrift

6-Chloro-5-vinylindoline (D62) (0.13 g, crude) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The crude product was recrystallised from ethanol/diethyl ether to give the title compound (22 mg) as a yellow crystalline solid m.p. 195°-200° C.

Quelle