Reaktion #443246

Reaktionsgleichung

6-Chloro-5-isopropylindoline

3-pyridylisocyanate

→

title compound

Ausbeute 57.0%

6-Chloro-5-isopropyl-1-(3-pyridylcarbamoyl)indoline

Ausbeute 57.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe product was recrystallised from ethanol/diethyl ether

Vorschrift

6-Chloro-5-isopropylindoline (D58) (0.4 g, 2.05 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The product was recrystallised from ethanol/diethyl ether to give the title compound (0.36 g, 57%) as a white crystalline solid m.p.=183°-185° C.

Quelle