Reaktion #443239

Reaktionsgleichung

6-Chloro-5-methylthioindoline

3-pyridylisocyanate

→

title compound

Ausbeute 81.0%

6-Chloro-5-methylthio-1-(3-pyridylcarbamoyl)indoline

Ausbeute 81.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe crude product was recrystallised from ethanol/diethyl ether

Vorschrift

6-Chloro-5-methylthioindoline (D48) (0.70 g, 3.51 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The crude product was recrystallised from ethanol/diethyl ether to give the title compound (0.91 g, 81%) as a white crystalline solid m.p. 241°-242° C.

Quelle