Reaktion #441797

ord-e09209f8f04a479ea087e9d9e99d0b36

Reagenzien

Keine

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The identical reduction of o-nitrotoluene as described in Example 3 was performed only the ethanol was eliminated. This reduction resulted in the isolation of a 48% yield of o-hydrazotoluene. Although the o-hydrazotoluene has a good solubility in tetrahydrofuran, the absence of ethanol prohibits the necessary level of sodium hydroxide from being dissolved in the reactive phase.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04375559uspto-grants-1983_03