Reaktion #441779

ord-33bc60857ac645f1a3e3a467526a3167

Reaktionsgleichung

Cl[Si](Cl)(c1ccccc1)c1ccccc1
diphenyldichlorosilane
COC(=O)Oc1nc(Cl)c(Cl)cc1Cl
methyl 3,5,6-trichloro-2-pyridyl carbonate
Clc1cc(Cl)c(O[Si](Oc2nc(Cl)c(Cl)cc2Cl)(c2ccccc2)c2ccccc2)nc1Cl
diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

In the manner described in Examples 1-7, diphenyldichlorosilane was reacted with about two moles of methyl 3,5,6-trichloro-2-pyridyl carbonate in the presence of tetrabutylammonium chloride to produce a good yield of diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane, a crystalline solid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04375549uspto-grants-1983_03