Reaktion #44056

ord-f9cd5bdb190940388027765a82ba36a1

Reaktionsgleichung

CS(=O)(=O)OCCc1cccc([N+](=O)[O-])c1
D4
CS(=O)(=O)OCCc1cccc([N+](=O)[O-])c1
2-(3-Nitrophenyl)ethyl methanesulfonate
OCCc1cccc(Br)c1
2-(3-bromophenyl)ethanol
→
CS(=O)(=O)OCCc1cccc(Br)c1
title compound
Ausbeute 77.0%
CS(=O)(=O)OCCc1cccc(Br)c1
2-(3-Bromophenyl)ethyl methanesulfonate
Ausbeute 77.0%

Edukte

CS(=O)(=O)OCCc1cccc([N+](=O)[O-])c1
D4
CS(=O)(=O)OCCc1cccc([N+](=O)[O-])c1
2-(3-Nitrophenyl)ethyl methanesulfonate
OCCc1cccc(Br)c1
2-(3-bromophenyl)ethanol

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared in 77% yield using a similar procedure to description D4 starting from 2-(3-bromophenyl)ethanol.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07732600B2uspto-grants-2010_06