Reaktion #439139

Reaktionsgleichung

4-hydroxyacetophenone

3-aminopropyltriethoxysilane

paraformaldehyde

→

final product

Ausbeute 55.0%

Benzoxazine

Ausbeute 55.0%

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound was prepared

Vorschrift

This compound was prepared according to the method used for the previous examples by combining 4-hydroxyacetophenone (13.6 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The final product was a clear, almost colorless liquid. The yield was 55%.

Quelle