Reaktion #439138

ord-ccafa9c809e64946a0be199b17c9234d

Reaktionsgleichung

O=C1C=CC(=O)N1c1ccc(O)cc1
4-maleimidophenol
CCO[Si](CCCN)(OCC)OCC
3-aminopropyltriethoxysilane
C=O
paraformaldehyde
C1=Cc2ccccc2ON1
final product
Ausbeute 37.0%
C1=Cc2ccccc2ON1
Benzoxazine
Ausbeute 37.0%

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound was prepared

Vorschrift

This compound was prepared according to the method used for the previous examples by combining 4-maleimidophenol (18.9 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The final product was a highly viscous red liquid. The yield was 37%.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06743852B2uspto-grants-2004_06