Reaktion #439133

ord-63dde14dd6d043aeb066dd2e0f91cd0f

Reaktionsgleichung

CCO[Si](CCCN)(OCC)OCC
3-aminopropyltriethoxysilane
Oc1ccc(O)cc1
hydroquinone
C1=Cc2ccccc2ON1
final product
Ausbeute 65.0%
C1=Cc2ccccc2ON1
Benzoxazine
Ausbeute 65.0%

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound was prepared

Vorschrift

This compound was prepared according to the method described previously using 3-aminopropyltriethoxysilane (22.1 g, 100 mmole), paraformaldehade (6.3 g, 210 mmole), hydroquinone (5.5 g, 50 mmole), and toluene (150 ml). The final product was a viscous liquid. The yield was 65% of theory.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06743852B2uspto-grants-2004_06