Reaktion #439132

ord-6358ad625d7f4fa781932705f29eec87

Reaktionsgleichung

CO[Si](CCCN)(OC)OC
3-aminopropyltrimethoxysilane
C=CCc1ccccc1O
2-allyl-phenol
C1=Cc2ccccc2ON1
final product
Ausbeute 94.0%
C1=Cc2ccccc2ON1
Benzoxazine
Ausbeute 94.0%

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound was prepared

Vorschrift

This compound was prepared according to the method described in the previous examples using 3-aminopropyltrimethoxysilane (17.9 g, 100 mmole), paraformaldehade (6.3 g, 210 mmole), 2-allyl-phenol (13.4 g, 0.1 mmole), and toluene (200 ml). The final product was obtained as a slightly yellow, mobile liquid. The yield was 94% of theory.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06743852B2uspto-grants-2004_06