Reaktion #439131

ord-c81baa594f844ee78f8115874d64300c

Reaktionsgleichung

CO[Si](CCCN)(OC)OC
3-aminopropyltrimethoxysilane
C=O
paraformaldehyde
Oc1cccc2ccccc12
1-naphthol
C1=Cc2ccccc2ON1
final product
Ausbeute 80.0%
C1=Cc2ccccc2ON1
Benzoxazine
Ausbeute 80.0%

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound was prepared

Vorschrift

This compound was prepared according to the method described in previous examples using 3-aminopropyltrimethoxysilane (17.9 g, 100 mmole), paraformaldehyde (6.3 g, 210 mmole), 1-naphthol (14.4 g, 100 mmole), and toluene (200 ml). The final product was obtained as a viscous liquid. The yield was 80% of theory.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06743852B2uspto-grants-2004_06