Reaktion #433164

Reaktionsgleichung

cyanuric chloride

2,2,6,6-tetramethyl-4-benzoyloxypiperidine

→

2,4-Dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine

Lösungsmittel

xylene

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeAfter recrystallization from isopropanol, 2,4-dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine
2. 2
   Sonstigeare obtained as colorless crystals

Vorschrift

46.1 g of cyanuric chloride and 136.0 g of 2,2,6,6-tetramethyl-4-benzoyloxypiperidine are reacted in 300 ml of xylene as described in Example 1 and worked up. After recrystallization from isopropanol, 2,4-dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine are obtained as colorless crystals having a melting point of 145°.

Quelle