Reaktion #430636

Reaktionsgleichung

phenylpropyl malonate

2-(2-iodophenyl)ethyl bromide

4-chlorobiphenyl

→

title compound

2-(2-Iodophenyl)ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe final product was recrystallized from chloroform
2. 2
   Sonstigeto give a fluffy, white solid (mp
3. 3
   Sonstigestarting at 50° C.

Vorschrift

The title compound was synthesized by a sequence similar to that for Example 87 except that 2-(2-iodophenyl)ethyl bromide and commercially available diethyl phenethyl malonate were used in lieu of the 4-chlorobiphenyl and phenylpropyl malonate respectively. The final product was recrystallized from chloroform to give a fluffy, white solid (mp: melts/softens over a broad range starting at 50° C.; the bulk of the sample melts at 189°-190° C.).

Quelle