Reaktion #430442

ord-6ebb58d68c9b47519f37846f8b70b865

Reaktionsgleichung

COC(=O)Oc1ccc(C(=O)O)cc1
compound 15
COC(=O)Oc1ccc(C(=O)O)cc1
4-methoxycarbonyloxybenzoic acid
O=C(O)c1ccc(O)cc1F
2-fluoro-4-hydroxybenzoic acid
COC(=O)Cl
methylchloroformate
COC(=O)Oc1ccc(C(=O)O)c(F)c1
2-fluoro-4-methoxycarbonyloxybenzoic acid

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis was prepared

Vorschrift

This was prepared using a similar method to that described for compound 15. Quantities: 2-fluoro-4-hydroxybenzoic acid (26) (0.97 g, 6.23 mmol), methylchloroformate (1.09 g, 11.48 mmol).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05861109uspto-grants-1999_01