Reaktion #429176

ord-28632a5e3c9f4f48846835d443b176f6

Reaktionsgleichung

CC(C)[C@H](N)CO
(S)-(+)-2-amino-3-methyl-1-butanol
CCOC(=O)OCC
diethyl carbonate
O=C([O-])[O-].[K+].[K+]
K2CO3
→
CC(C)[C@H]1COC(=O)N1
title compound
CC(C)[C@H]1COC(=O)N1
4-(S)-(1-Methylethyl)-2-oxazolidinone

Edukte

CC(C)[C@H](N)CO
(S)-(+)-2-amino-3-methyl-1-butanol
CCOC(=O)OCC
diethyl carbonate
O=C([O-])[O-].[K+].[K+]
K2CO3

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared according to Evans, Mathre and Scott (J. Org. Chem., 50, 1830 (1985)) from (S)-(+)-2-amino-3-methyl-1-butanol and diethyl carbonate in the presence of K2CO3.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05856322uspto-grants-1999_01