Reaktion #428209

ord-303eacb95df640eab0cb79342a9560db

Reaktionsgleichung

Clc1nc(Cl)nc(Cl)n1
cyanuryl chloride
CCCCC(CC)CN
2-ethyl-1-hexylamine
CCCCC(CC)CN=c1nc(Cl)nc(Cl)[nH]1
2,4-bischloro-6-(2-ethylhexyl)imino-1,3,5-triazine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Similarly to the process reported in example 1, the cyanuryl chloride was reacted with 2-ethyl-1-hexylamine, to obtain the corresponding intermediate 2,4-bischloro-6-(2-ethylhexyl)imino-1,3,5-triazine. Similarly to the process reported in examples 2 and 3, the latter was reacted with two equivalents of p-aminobenzoic acid to give the corresponding diacid, which was then converted to the corresponding diacyl chloride by the action of thionyl chloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08895731B2uspto-grants-2014_11