Reaktion #42728

Reaktionsgleichung

4-iodophenylacetic acid

hydrochloric acid

MeOH

→

title compound

Ausbeute 98.0%

Methyl 4-Iodophenylacetate

Ausbeute 98.0%

Lösungsmittel

dioxane

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe solvent was removed under reduced pressure

Vorschrift

To a stirred solution of 4-iodophenylacetic acid (5.0 g, 19.1 mmol) in MeOH (200 mL) was added 4N hydrochloric acid in dioxane (10 mL). The reaction mixture was stirred for 24 h at room temperature and then the solvent was removed under reduced pressure to give the title compound (5.17 g, 98% yield), which was used without further purification.

Quelle