Reaktion #42627

ord-b079a0f2f802400692410169afbb905d

Reaktionsgleichung

CCC(C)NC(=O)C=CC(=O)OC
methyl 3-(sec-butylcarbamoyl)acrylate
NCCCCCCO
6-amino-1-hexanol
CCC(C)NC(=O)CC(NCCCCCCO)C(=O)OC
desired product
CCC(C)NC(=O)CC(NCCCCCCO)C(=O)OC
Methyl 3-(sec-butylcarbamoyl)-2-(6-hydroxyhexylamino)propanoate

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

To methyl 3-(sec-butylcarbamoyl)acrylate from the above reaction at room temperature was added the 6-amino-1-hexanol (13.7 g, 117 mmol) and the resulting mixture was stirred overnight to give the desired product.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07732018B2uspto-grants-2010_06