Reaktion #4254

Reaktionsgleichung

decyl p-aminobenzoate

cyanuric chloride

hydrogen chloride

→

1,3,5-Tris-(p-(dec-1-yloxycarbonyl)-anilino)-s-triazine

Lösungsmittel

xylene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Waschenwashed twice with saturated sodium bicarbonate solution and once with water
2. 2
   Temperaturcooled to room temperature
3. 3
   SonstigeThe white crystals precipitated
4. 4
   Filtrationwere filtered off under suction
5. 5
   Sonstigedried

Vorschrift

83 g of decyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The white crystals precipitated were filtered off under suction and dried.

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