Reaktion #42146

ord-0b6a244a31ae4bdea68240493807b244

Reaktionsgleichung

CCCCP(CCCC)CCCC
Tri-n-butylphosphine
Cl
hydrochloric acid
[Na+].c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
sodium tetraphenylborate
→
CCCC[PH+](CCCC)CCCC.c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
tri-n-butylphosphonium tetraphenylborate
Ausbeute 53.0%

Edukte

CCCCP(CCCC)CCCC
Tri-n-butylphosphine
Cl
hydrochloric acid
[Na+].c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
sodium tetraphenylborate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Tri-n-butylphosphine is reacted with hydrochloric acid in the presence of sodium tetraphenylborate to produce tri-n-butylphosphonium tetraphenylborate (53% yield) (see Nonpatent Document 6).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07728176B2uspto-grants-2010_06