Reaktion #42090

Reaktionsgleichung

1-(2-chlorophenyl)-2-(4-chlorophenyl)ethanone

N,N-dimethyformamide dimethyl acetal

→

1-(2-Chlorophenyl)-2-(4-chlorophenyl)-3-(dimethylamino)prop-2-en-1-one

Lösungsmittel

DMF

Reaktionsbedingungen

Aufarbeitung

1. 1
   EinengenThe solution was then concentrated
2. 2
   Sonstigeused without further purification in the next step

Vorschrift

To 13.2 g of 1-(2-chlorophenyl)-2-(4-chlorophenyl)ethanone in 100 mL of DMF was added 23.8 g of N,N-dimethyformamide dimethyl acetal. The mixture was stirred at 75° C. for 16 hours. The solution was then concentrated and used without further purification in the next step.

Quelle