Reaktion #42032

Reaktionsgleichung

3,5-dichloro-4-methylbenzoic acid

methanol

→

methyl 3,5-dichloro-4-methylbenzoate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethat the crude product was purified by silica gel column chromatography

Vorschrift

This compound was prepared in the same manner as in Reference Example 1 (step 1), except that 3,5-dichloro-4-methylbenzoic acid (Japanese Unexamined Patent Publication (Kokai) No. 6-192196) was used and methanol was used as the solvent, and that the crude product was purified by silica gel column chromatography.

Quelle