Reaktion #420226

ord-abb4262e97d54faf827a7f99a518c7dd

Reaktionsgleichung

CN(C)CC(C)(C)C=O
2,2-dimethyl-3-dimethylaminopropanal
CC(C)N
2-propanamine
CCO[Si](CCCN)(OCC)OCC
3-aminopropyltriethoxysilane
CCO[Si](CCCN=CC(C)(C)CN(C)C)(OCC)OCC
3-(2,2-Dimethyl-3-(N,N-dimethylamino)propylideneamino)propyltriethoxysilane

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

13.57 g 2,2-dimethyl-3-dimethylaminopropanal, 7.45 g 2-propanamine and 22.14 g 3-aminopropyltriethoxysilane were reacted according to the general manufacturing procedure (iminosilanes). Yield: 32.3 g of a clear, colorless oil having an amine content of 5.97 mmol N/g and a purity of 98%.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08877955B2uspto-grants-2014_11