Reaktion #420225

Reaktionsgleichung

2,2-dimethyl-3-dimethylaminopropanal

2-propanamine

3-aminopropyltrimethoxysilane

→

3-(2,2-dimethyl-3-(N,N-dimethylamino)propylideneamino)propyltrimethoxysilane

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.DISTILLATIONThe product was distilled after manufacture in order
2. 2
   Sonstigeto remove oligomer portions

Vorschrift

13.57 g 2,2-dimethyl-3-dimethylaminopropanal, 7.45 g 2-propanamine and 17.93 g 3-aminopropyltrimethoxysilane were reacted according to the general manufacturing procedure (iminosilanes). The product was distilled after manufacture in order to remove oligomer portions. Yield: 28.4 g of a clear, colorless oil having an amine content of 6.61 mmol N/g and a purity of 95%.

Quelle