Reaktion #42014

Reaktionsgleichung

sodium bromate

4-fluorobenzyl alcohol

→

4-fluorobenzoic acid

Ausbeute 89.7%

Lösungsmittel

acetonitrile water

Reaktionsbedingungen

Vorschrift

The separated catalyst was added to a fresh batch of sodium bromate (0.3 g) and 4-fluorobenzyl alcohol (0.256 g, 2 mmol) in acetonitrile:water (1:1, 10 ml). The above procedure was repeated to give 4-fluorobenzoic acid as a white solid (0.25 g, 88%).

Quelle