Reaktion #42011

Reaktionsgleichung

ethyl oleate

pentanol

→

pentyl oleate

Ausbeute 91.0%

Lösungsmittel

ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwas refluxed
2. 2
   workup.ADDITIONwas added
3. 3
   Filtrationthe catalyst was filtered off
4. 4
   Einengenconcentrated

Vorschrift

A mixture containing Catalyst A or B (0.05 g) and ethyl oleate (1.55 g, 5 mmol) and pentanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give pentyl oleate as an oil (1.6 g, 91% yield).

Quelle