Reaktion #42009

Reaktionsgleichung

oleic acid

ethanol

→

ethyl oleate

Ausbeute 90.0%

Lösungsmittel

ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwas refluxed
2. 2
   workup.ADDITIONwas added
3. 3
   Filtrationthe catalyst was filtered off
4. 4
   Einengenconcentrated

Vorschrift

A mixture containing Catalyst A (0.05 g) and oleic acid (1.41 g, 5 mmol) and ethanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give ethyl oleate as an oil (1.39 g, 90% yield).

Quelle