Reaktion #417934

Reaktionsgleichung

phenol

3-o-tolylpropanoyl chloride

→

product

Ausbeute 93.0%

Phenyl 3-(o-tolyl)propanoate

Ausbeute 93.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.DISTILLATIONdistilled at 127-129° C./0.05 mbar

Vorschrift

The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.

Quelle