Reaktion #415742

ord-b20a6d4cdab24044b85bc4f29bad8363

Reaktionsgleichung

[Al+3].[OH-].[OH-].[OH-]
aluminum hydroxide
O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Al+3].[Al+3]
aluminum sulfate
NCC(=O)O
glycine
O=C([O-])[O-].[Mg+2]
magnesium carbonate
O=[N+]([O-])[O-]
nitrate
NCC(=O)[O-].NCC(=O)[O-].[Mg+2]
Magnesium glycinate

Lösungsmittel

Reaktionsbedingungen

Temperatur
75°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigethe mixture was reacted with agitation at 75° C. for 1/2 hour
  2. 2
    Sonstigeoven dried at 58° C. under a vacuum of 328 mm of Hg

Vorschrift

Magnesium glycinate was prepared by reacting 5 grams of glycine with 3.1 grams of basic magnesium carbonate (26.3% Mg) in 15 grams of water. The mixture was heated at 75° C. for 1/2 hour with agitation. The hot solution was then added to 113 grams of zirconyl nitrate (7.9% Zr) with stirring. After the addition of 1.5 grams of aluminum hydroxide powder (28.8% Al), the mixture was reacted with agitation at 75° C. for 1/2 hour. To the resultant clear solution was added 7.9 grams of 2/3 basic aluminum sulfate, Al(OH)2SO4 (3.1% Al). The solution was then oven dried at 58° C. under a vacuum of 328 mm of Hg. The product contained 1.2% Mg, 13.2% glycine, 1.5% Al, 24.3% Zr, 4.02% SO4 and 29.5% nitrate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04017599uspto-grants-1977_04