Reaktion #414660

Reaktionsgleichung

t-butyl 4-(bromomethyl)-1H-benzimidazole-1-carboxylate

diethyl (dipropylamino)malonate

→

5,6-Dihydro-N,N-dimethyl-4H-pyrrolo(3,2,1ij)quinolin-5-amine

Lösungsmittel

THF ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound was prepared

Vorschrift

This compound was prepared by following the procedure of Example 18, but substituting methyl 7-(bromomethyl)-1H-indole-1-carboxylate for t-butyl 4-(bromomethyl)-1H-benzimidazole-1-carboxylate and diethyl (dimethylamino)malonte for diethyl (dipropylamino)malonate. The bulk of the product was converted to the maleate salt, mp 114°-115° C. from THF/ether.

Quelle