Reaktion #412767

Reaktionsgleichung

p-Dioxanone

N-methyl-2,5- morpholinedione

1-dodecanol

stannous octoate

→

p-Dioxanone N-Methyl-2,5-Morpholinedione

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONmagnetically mixed in
2. 2
   Temperatura flame
3. 3
   Sonstigevacuum dried
4. 4
   Sonstigesealed glass ampule

Vorschrift

p-Dioxanone (28.5 g, 0.279 moles), N-methyl-2,5- morpholinedione (1.5 g, 0.01162 moles), 1-dodecanol (0.082 g, 0.00044 moles), and a catalytic amount of stannous octoate (0.06 ml of a 0.33 M toluene solution, 0.0000198 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampule according to the following temperature/time scheme:

Quelle